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Factory Sells Best Quality 2,3-DIBROMO-3-PHENYLPROPIONIC ACID 6286-30-2 with GMP standards
- Molecular Formula: C9H8Br2O2
- Molecular Weight: 307.969
- Vapor Pressure: 0.000122mmHg at 25°C
- Melting Point: 200 °C (dec. )(lit. )
- Boiling Point: 321.5 °C at 760 mmHg
- PKA: 2.21±0.11(Predicted)
- Flash Point: 148.3 °C
- PSA： 37.30000
- Density: 1.914 g/cm3
- LogP: 2.97070
2,3-DIBROMO-3-PHENYLPROPIONIC ACID(Cas 6286-30-2) Usage
|
General Description |
Dehydrobromination of α,β-dibromohydrocinnamic acid has been studied in liquid ammonia. |
InChI:InChI=1/C9H8Br2O2/c10-7(8(11)9(12)13)6-4-2-1-3-5-6/h1-5,7-8H,(H,12,13)/p-1/t7-,8-/m1/s1
6286-30-2 Relevant articles
Catalyst-Free 1,2-Dibromination of Alkenes Using 1,3-Dibromo-5,5-dimethylhydantoin (DBDMH) as a Bromine Source
Wang, Lei,Zhai, Lele,Chen, Jinyan,Gong, Yulin,Wang, Peng,Li, Huilin,She, Xuegong
supporting information, p. 3177 - 3183 (2022/02/23)
A direct 1,2-dibromination method of alk...
Synthesis method of o-Dibromo compound
-
Paragraph 0042-0051, (2022/01/04)
The present invention discloses a synthe...
Chemical validation of a druggable site on Hsp27/HSPB1 using in silico solvent mapping and biophysical methods
Makley, Leah N.,Johnson, Oleta T.,Ghanakota, Phani,Rauch, Jennifer N.,Osborn, Delaney,Wu, Taia S.,Cierpicki, Tomasz,Carlson, Heather A.,Gestwicki, Jason E.
, (2021/02/09)
Destabilizing mutations in small heat sh...
Stable and Highly Regioselective Anionic Polymerization of (Z)-1-Phenyl[3]dendralene
Miya, Masamitsu,Takagi, Tsukasa,Takenaka, Katsuhiko,Toda, Tomoyuki
, p. 4326 - 4332 (2021/05/29)
The anionic polymerization of (Z)-1-phen...
6286-30-2 Process route
-
-
140-10-3
(E)-3-phenylacrylic acid
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-
6286-30-2
2,3-dibromo-3-phenylpropanoic acid
| Conditions | Yield |
|---|---|
|
With
bromine;
In
tetrachloromethane;
|
96.7%
|
|
With
bromine;
In
tetrachloromethane;
|
93%
|
|
With
sodium perborate; sodium bromide;
In
acetic acid;
for 2h;
|
90%
|
|
With
bromine;
In
chloroform;
for 0.5h;
Reflux;
|
83%
|
|
With
bromine;
In
tetrachloromethane;
|
47%
|
|
With
bromine;
at 20 ℃;
for 168000h;
under 165 Torr;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
for 2h;
|
21 g
|
|
With
bromine;
In
acetic acid;
for 2h;
Inert atmosphere;
|
-
-
621-82-9
Cinnamic acid
-
-
6286-30-2
2,3-dibromo-3-phenylpropanoic acid
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride;
In
dichloromethane; water;
at 20 - 45 ℃;
|
88%
|
|
With
propane 3-bromo-1-(triphenylphosphonium) tribromide;
In
dichloromethane;
at 20 ℃;
for 2h;
|
85%
|
|
With
potassium bromate; LACTIC ACID; cerium(IV) sulphate; sulfuric acid;
In
water; benzene;
at 36.5 ℃;
Mechanism;
Irradiation;
oscillatory characteristics oscillatory reaction, also in dark;
|
|
|
With
water; bromine;
|
|
|
With
sulfurous dibromide;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
for 1h;
|
11.5 g
|
|
With
bromine;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
for 0.333333h;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
Sealed tube;
|
|
|
With
bromine;
In
chloroform;
at 0 ℃;
|
|
|
With
bromine;
In
chloroform;
for 0.333333h;
Cooling with ice;
Inert atmosphere;
Schlenk technique;
|
6286-30-2 Upstream products
-
67-66-3
chloroform
-
140-10-3
cis-cinnamic acid
-
621-82-9
Cinnamic acid
-
140-10-3
(E)-3-phenylacrylic acid
6286-30-2 Downstream products
-
15813-24-8
(Z)-2-bromo-3-phenylacrylic acid
-
621-82-9
Cinnamic acid
-
21770-48-9
methyl 2,3-dibromo-3-phenylpropanoate
-
588-72-7
[(E)-2-bromoethenyl]benzene
