Cost-effective customized wholesale 3-Hydroxy-1-methylpropyl acetate 75355-65-6
- Molecular Formula: C6H12O3
- Molecular Weight: 132.159
- Vapor Pressure: 2.25mmHg at 25°C
- Refractive Index: 1.427
- Boiling Point: 142.6 °C at 760 mmHg
- PKA: 14.84±0.10(Predicted)
- Flash Point: 41.7 °C
- PSA： 46.53000
- Density: 1.024 g/cm3
- LogP: 0.32040
3-Hydroxy-1-methylpropyl acetate(Cas 75355-65-6) Usage
InChI:InChI=1/C6H12O3/c1-5(3-4-7)9-6(2)8/h5,7H,3-4H2,1-2H3
75355-65-6 Relevant articles
Sulfonic acid-functionalized periodic mesoporous organosilicas in esterification and selective acylation reactions
Karimi, Babak,Mirzaei, Hamid M.,Mobaraki, Akbar,Vali, Hojatollah
, p. 3624 - 3631 (2015/07/01)
The application of sulfonic acid-functio...
Gold(I)/copper(II)-cocatalyzed tandem cyclization/semipinacol reaction: Construction of 6-Aza/Oxa-Spiro[4.5]decane skeletons and formal synthesis of (±)-halichlorine
Zhu, Dao-Yong,Zhang, Zhen,Mou, Xue-Qing,Tu, Yong-Qiang,Zhang, Fu-Min,Peng, Jin-Bao,Wang, Shao-Hua,Zhang, Shu-Yu
supporting information, p. 747 - 752 (2015/03/18)
A simple and efficient strategy for the ...
Simple and practical method for selective acylation of primary hydroxy group catalyzed by N-methyl-2-phenylimidazole (Ph-NMI) or 2-phenylimidazo[2,1-b]benzothiazoles (Ph-IBT)
Ibe, Kouta,Hasegawa, Yu-Suke,Shibuno, Misuzu,Shishido, Tsukasa,Sakai, Yuzo,Kosaki, Yu,Susa, Keisuke,Okamoto, Sentaro
, p. 7039 - 7042 (2015/01/08)
N-Methyl-2-phenylimidazole (Ph-NMI) and ...
A highly selective, high-speed, and hydrolysis-free O-acylation in subcritical water in the absence of a catalyst
Sato, Masahiro,Matsushima, Keiichiro,Kawanami, Hajime,Ikuhsima, Yutaka
, p. 6284 - 6288 (2008/04/05)
(Chemical Equation Presented) Fast and f...
75355-65-6 Process route
-
-
18826-95-4,107-88-0
1.3-butanediol
-
-
108-24-7
acetic anhydride
-
-
1851-86-1
butane-1,3-diol 1-acetate
-
-
1117-31-3
1,3-diacetoxybutane
-
-
75355-65-6
3-hydroxy-1-methylpropyl acetate
| Conditions | Yield |
|---|---|
|
With
sodium hydride;
|
|
|
With
CoCl2;
In
acetonitrile;
at 80 ℃;
for 2h;
under 750.075 Torr;
Title compound not separated from byproducts.;
|
21 % Chromat.
|
-
-
18826-95-4,107-88-0
1.3-butanediol
-
-
108-24-7
acetic anhydride
-
-
1851-86-1
butane-1,3-diol 1-acetate
-
-
75355-65-6
3-hydroxy-1-methylpropyl acetate
| Conditions | Yield |
|---|---|
|
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
|
75355-65-6 Upstream products
-
766-20-1
2,4-dimethyl-[1,3]dioxane
-
1117-31-3
1,3-diacetoxybutane
-
18826-95-4
1.3-butanediol
-
108-24-7
acetic anhydride
